Das Einbindungsverhalten von Alkaliverbindungen in Additive beim Einsatz von Biomassen in Staubfeuerungen

Thesis from Björn Beeh
University of Stuttgart, 2024

The rising global demand for energy and the increasing discussion about saving 
carbon dioxide in the generation of heat and electrical energy are bringing conventional 
power plants, where energy is generated from fossil fuels, into focus. The decision by 
politicians to phase out nuclear power and the generation of electricity from coal is 
making the supply situation in many parts of Germany more difficult. 
Renewable energies such as the use of solar and wind power can only close this gap 
to a limited extent without suitable storage solutions due to the fluctuation of the energy 
supply over time. In addition, the large wind farms that have the potential to replace 
coal-fired power plants are mainly located at the coasts in northern Germany. However, 
due to the lack of distribution grid capacity, the energy generated here cannot be 
transported to industrial centers such as those in the Ruhr region and southern 
Germany. 
It therefore makes sense to convert the existing coal-fired plants, which will be deprived 
of their operating basis by the planned phase-out of coal-fired power generation, to 
biomass. 
Due to the large amounts of fuel needed as well as the dust firing technology in use, 
not every biomass is suitable. The decisive factors are availability, energy density as 
well their usability in a dust firing system. Pellets made of wood and agricultural 
residues such as sunflower husks have proven to be promising, due to their energy 
density, which is comparable to dry lignite. 
Due to the location of coal-fired power plants at the coast or near rivers, which have 
already been used to transport coal, the logistics for transporting biomass in the form 
of pellets are already in place. 
The necessary modifications to the existing power plant units are mainly limited to fuel 
preparation. Here, adapted fuel mills are needed to break down the bond of the 
biomass fiber in the pellet again. 
The use of biomass in conventional pulverized fuel furnaces offers the advantage that 
the fuel is considered CO2-neutral, since the amounts released correspond to what the 
plants have sequestered from the atmosphere during their growth. In addition, the use 
of biomass leads to a significant reduction in the ash mass flows resulting from the 
combustion process. 
Additional to the advantages, the use of biomasses also entails various disadvantages. 
For example, most biomasses contain significantly higher concentrations of phosphor 
and alkali metals, which cause damage and higher operating costs in the area of the 
furnace and the boiler, due to corrosion, and also have negative effects in the 
downstream units of the flue gas cleaning system. This applies in particular to the SCRDeNOx-catalyst, in the following named DeNOx-catalyst, which is installed in most 
pulverized fuel furnaces to reduce nitrogen oxides from the combustion process. This 
catalyst usually consists of a matrix of titanium dioxide doped with active components 
such as vanadium pentoxide. Phosphorus compounds, for example, cause sticky 
coating in the pores and thus reduce the catalyst surface. However, this process is 
reversible with appropriate measures. In contrast, catalyst deactivation caused by 
potassium compounds is not reversible. 
For this reason, this work deals with the influence of additives added to the combustion 
process to reduce the negative effects on the catalyst. There are various approaches 
to this in literature, but in this work the approach of incorporation into alumino-silicate 
structures is investigated based on experimental tests. 
The work is divided into three parts, starting with the characterization of fuels and 
additives on a laboratory scale. In the second part, based on the data from the 
investigations carried out in the first part, calculations are performed using FactSageTM
on the release or incorporation behavior of the alkali compounds. The third part of the 
work is followed by investigations on an entrained-flow reactor as well as a dust furnace 
in order to verify the statements of the second part of the work under real conditions. 
In addition to the analyses carried out directly during the test series, such as emission 
measurements, ash and catalyst samples were also examined and evaluated 
subsequently using a scanning electron microscope. 
The investigations show that the use of alumino-silicate-based additives results in rapid 
and stable incorporation of the potassium bound in the fuel in the combustion reaction 
zone. 
In addition, it has been shown that chlorine compounds also present in the fuel lead to 
an increased HCl concentration in the combustion waste gas due to the lack of 
potassium as a reaction partner. In addition to emission problems, this can lead to 
corrosion with metallic materials, if the acid dew point is undershot. 
The findings obtained from the test series show that, if aluminosilicate-based additives 
are used, the formation of potassium chloride during the thermal conversion of the 
biomasses investigated, can be significantly reduced and the potassium can be stably 
incorporated into the additive. 

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